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All records

ENV-2026-04429

In reviewEnvironmental

Sediment Core — Reach 2

Route for review Add to report
78Integrity

2

Findings

1

Critical

0

Cleared

Method
EPA 537.1 — PFAS by LC-MS/MS
Instrument
PerkinElmer NexION 2000
Analyst
S. Ahmadi
Sample ID
ENV-S39183
Batch
B-2265
Source
LIMS_export_2026-06.csv
Collected
Jun 10, 2026
Scanned
Jun 23, 2026

ALCOA+ findings (2)

Confidence85%Fieldperformed_by AI-assisted · human sign-off required
Why flagged
The result was recorded without a verified analyst identity. Records that cannot be traced to a specific, authenticated user fail the Attributable principle and are not defensible during inspection.
Source evidence
Instrument session 7900-S4421 has no logged operator for this acquisition.
Suggested remediation
Re-associate the entry with the authenticated analyst from the instrument session log, or obtain a documented attribution statement countersigned by the QA Manager.
Reviewer decision
Awaiting a reviewer. No decision recorded yet.
Record history

Imported from LIMS_export_2026-06.csv

Jun 10, 2026, 02:20 PM

ALCOA+ integrity scan completed

Jun 23, 2026, 02:20 PM

Missing analyst attribution flagged (critical)

Jun 23, 2026, 02:20 PM

Manual integration without justification flagged (major)

Jun 23, 2026, 02:20 PM